Lab Report: Synthesis and Characterization of Adipic Acid by Yaghubi, Lab Reports of Organic Chemistry

Download Lab Report: Synthesis and Characterization of Adipic Acid by Yaghubi and more Lab Reports Organic Chemistry in PDF only on Docsity! Yaghubi 1 Green Synthesis of Adipic Acid Sahabe Yaghubi Professor Dr. Anness Organic Chemistry 231-0980 12/06/2021 Yaghubi 2 Yaghubi 5 Analysis 1. Provide the final mass of product after recrystallization (show Calculation). Filter paper: 0.32 g Buncher Top: 33.44 g Mass of (Buncher Top+ filter paper + source) = 35.21 g Final mass = (mass of Buncher Top+filter paper + source) - (mass of Buncher Top + filter paper) Final mass of product = 35.21 g - (0.32g + 33.44 g) = 35.21 g-33.76g Determine the theoretical yield of the product (adipic acid) in grams and show all of your Calculations. (Note: This is done just like you learned in general chemistry starting with the mass of the limiting reactant and converting it to the mass of the product). 2.05 g cyclohexene * (1 mol cyclohexene/80.15 g cyclohexene) * (1 mol adipic acid/1 mol cyclohexene) * (146.14 g adipic acid/ 1 mol adipic acid) = 3.65g Determine the percent yield of the product (show calculation). % yield of the product ( 1.45/3.65 ) * 100 = 39.73% % yield of the product is 307% Provide the melting point range of the product. The melting point range of the product is M73 BIGOMIZ3EC. 5. Yaghubi 6 + Provide a table with important IR peaks for your product. The table should have two columns labeled bond type and wavenumber (cm-1). (Note: The IR spectrum of the product was provided during the lab session). Bond type Wavelength (cm-1)